Liquid hot water pretreatment of lignocellulosic biomass at lab and pilot scale

Jose M. Jimenez-Gutierrez; Rob A.J. Verlinden; Peter C. van der Meer; Luuk A.M. van der Wielen; Adrie J.J. Straathof

doi:10.3390/pr9091518

Liquid hot water pretreatment of lignocellulosic biomass at lab and pilot scale

Jose M. Jimenez-Gutierrez, Rob A.J. Verlinden, Peter C. van der Meer, Luuk A.M. van der Wielen, Adrie J.J. Straathof

Department of Chemical Sciences

Research output: Contribution to journal › Article › peer-review

Abstract

Liquid hot water pretreatment is considered to be a promising method for increaing biomass digestibility due to the moderate operational conditions without chemical additionA necessary step towards the scalability of this pretreatment process is performing pilot plant triaUpscaling was evaluated with a scaling factor of 500, by using 50 mL in the laboratory and 25 L in pilot plant batch reactor. Pretreatment times were varied from 30 to 240 min, and temperatures usewere 180–188^◦ C, while applying similar heating profiles at both scales. The initial mass fraction poplar wood chips ranged from 10% to 16%. Liquid hot water pretreatment at laboratory and pilscale led to analogous results. The acetic acid analysis of the liquid and solid fractions obtained aftpretreatment indicated that complete deacetylation of poplar biomass can be achieved.

Original language	English
Article number	1518
Journal	Processes
Volume	9
Issue number	9
DOIs	https://doi.org/10.3390/pr9091518
Publication status	Published - Sep 2021

Keywords

Autohydrolysis
Biorefinery
Lignocellulosic biomass
Liquid hot water
Pilot plant
Pretreatment

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10.3390/pr9091518

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title = "Liquid hot water pretreatment of lignocellulosic biomass at lab and pilot scale",

abstract = "Liquid hot water pretreatment is considered to be a promising method for increaing biomass digestibility due to the moderate operational conditions without chemical additionA necessary step towards the scalability of this pretreatment process is performing pilot plant triaUpscaling was evaluated with a scaling factor of 500, by using 50 mL in the laboratory and 25 L in pilot plant batch reactor. Pretreatment times were varied from 30 to 240 min, and temperatures usewere 180–188◦ C, while applying similar heating profiles at both scales. The initial mass fraction poplar wood chips ranged from 10% to 16%. Liquid hot water pretreatment at laboratory and pilscale led to analogous results. The acetic acid analysis of the liquid and solid fractions obtained aftpretreatment indicated that complete deacetylation of poplar biomass can be achieved.",

keywords = "Autohydrolysis, Biorefinery, Lignocellulosic biomass, Liquid hot water, Pilot plant, Pretreatment",

author = "Jimenez-Gutierrez, {Jose M.} and Verlinden, {Rob A.J.} and {van der Meer}, {Peter C.} and {van der Wielen}, {Luuk A.M.} and Straathof, {Adrie J.J.}",

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doi = "10.3390/pr9091518",

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volume = "9",

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TY - JOUR

T1 - Liquid hot water pretreatment of lignocellulosic biomass at lab and pilot scale

AU - Jimenez-Gutierrez, Jose M.

AU - Verlinden, Rob A.J.

AU - van der Meer, Peter C.

AU - van der Wielen, Luuk A.M.

AU - Straathof, Adrie J.J.

PY - 2021/9

Y1 - 2021/9

N2 - Liquid hot water pretreatment is considered to be a promising method for increaing biomass digestibility due to the moderate operational conditions without chemical additionA necessary step towards the scalability of this pretreatment process is performing pilot plant triaUpscaling was evaluated with a scaling factor of 500, by using 50 mL in the laboratory and 25 L in pilot plant batch reactor. Pretreatment times were varied from 30 to 240 min, and temperatures usewere 180–188◦ C, while applying similar heating profiles at both scales. The initial mass fraction poplar wood chips ranged from 10% to 16%. Liquid hot water pretreatment at laboratory and pilscale led to analogous results. The acetic acid analysis of the liquid and solid fractions obtained aftpretreatment indicated that complete deacetylation of poplar biomass can be achieved.

AB - Liquid hot water pretreatment is considered to be a promising method for increaing biomass digestibility due to the moderate operational conditions without chemical additionA necessary step towards the scalability of this pretreatment process is performing pilot plant triaUpscaling was evaluated with a scaling factor of 500, by using 50 mL in the laboratory and 25 L in pilot plant batch reactor. Pretreatment times were varied from 30 to 240 min, and temperatures usewere 180–188◦ C, while applying similar heating profiles at both scales. The initial mass fraction poplar wood chips ranged from 10% to 16%. Liquid hot water pretreatment at laboratory and pilscale led to analogous results. The acetic acid analysis of the liquid and solid fractions obtained aftpretreatment indicated that complete deacetylation of poplar biomass can be achieved.

KW - Autohydrolysis

KW - Biorefinery

KW - Lignocellulosic biomass

KW - Liquid hot water

KW - Pilot plant

KW - Pretreatment

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U2 - 10.3390/pr9091518

DO - 10.3390/pr9091518

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VL - 9

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ER -

Liquid hot water pretreatment of lignocellulosic biomass at lab and pilot scale

Abstract

Keywords

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