Parameters affecting pressureless sintering of α'-Sialons with lanthanide modifying cations

K. P.J. O'Reilly, M. Redington, S. Hampshire, M. Leigh

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Abstract

α-silicon nitride forms a range of solid solution Mx(Si, Al)12(O,N)16 where x = 2 and M is Li+, Ca2+, Y3+ or certain lanthanide cations. This paper reports the formation of Ln-α'-sialons by the reaction of Si3N4 with AlN and Ln2O3 where Ln = Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu and Y. Transformation reactions of Nd, Sm, Gd, Ho, Er and Y cations occurring during liquid phase pressureless sintering are reported. The effects of the volume and viscosity of the liquid phase and the amount of secondary N-melilite on sintering are discussed.

Original languageEnglish
Title of host publicationSilicon Nitride Ceramics, Scientific and Technological Advances
PublisherPubl by Materials Research Society
Pages393-398
Number of pages6
ISBN (Print)1558991824
Publication statusPublished - 1993
EventMaterials Research Society Fall Meeting - Boston, MA, USA
Duration: 1 Dec 19923 Dec 1992

Publication series

NameMaterials Research Society Symposium Proceedings
Volume287
ISSN (Print)0272-9172

Conference

ConferenceMaterials Research Society Fall Meeting
CityBoston, MA, USA
Period1/12/923/12/92

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