Stress evolution in electrodeposited copper metallization during room-temperature aging

T. Chowdhury, S. Ahmed, D. N. Buckley, M. T. Laugier, S. Nakahara, C. Heffernan

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

Abstract

Stress changes in electrodeposited copper films during room temperature aging were monitored by measuring the bending of the substrate using an optical fiber displacement sensor. Electrodeposition was carried out galvanostatically on evaporated copper films on borosilicate glass substrates in a stirred acidic copper sulphate bath at room temperature. It was observed that stress increases rapidly in the tensile direction reaching a plateau after ∼1 hour of room temperature aging. The magnitude of the change was observed to increase with increasing current density but to decrease with increasing film thickness. The effect of additives to the bath was investigated. Films deposited in the presence of added chloride ions subsequently showed an increased change in stress during room-temperature aging but the effect did not increase significantly with concentration. Films deposited with BTA as an additive also showed an increased change in stress during aging and the effect increased significantly with increasing concentration. The effect of added PEG was small while the addition of thiourea had a significant and complex effect. copyright The Electrochemical Society.

Original languageEnglish
Title of host publicationCopper Interconnects, New Contact and Barriers Metallurgies/Structures, and Low-k Interlevel Dielectrics III
PublisherElectrochemical Society Inc.
Pages93-103
Number of pages11
Edition11
ISBN (Electronic)9781566774994
DOIs
Publication statusPublished - 2006
EventCopper Interconnects, New Contact and Barrier Metallurgies/Structures, and Low-k Interlevel Dielectrics III - 208th Electrochemical Society Meeting - Los Angeles, CA, United States
Duration: 16 Oct 200521 Oct 2005

Publication series

NameECS Transactions
Number11
Volume1
ISSN (Print)1938-5862
ISSN (Electronic)1938-6737

Conference

ConferenceCopper Interconnects, New Contact and Barrier Metallurgies/Structures, and Low-k Interlevel Dielectrics III - 208th Electrochemical Society Meeting
Country/TerritoryUnited States
CityLos Angeles, CA
Period16/10/0521/10/05

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