X-ray crystal structure of trans-dinitratotetrapyridinezinc(II)-pyridine solvate, a clathrate compound

Pierre Losier; Michael J. Zaworotko

doi:10.1007/BF01677781

X-ray crystal structure of trans-dinitratotetrapyridinezinc(II)-pyridine solvate, a clathrate compound

Pierre Losier, Michael J. Zaworotko

Saint Mary's University Halifax

Research output: Contribution to journal › Article › peer-review

Abstract

The X-ray structure of trans-dinitratotetrapyridinezinc(II) · 2 pyridine has been determined. Clear colorless crystals of the complex crystallize in the orthorhombic space group Occa, with cell dimensions a = 12.108(3), b = 14.966(7) and c = 17.113(4)Å; V = 3101.0(18)Å³ and Z = 4. Unique reflections, 755, with I_net > 3σ (I) on refinement afforded values of R = 0.069 and R_w = 0.075.

Original language	English
Pages (from-to)	277-280
Number of pages	4
Journal	Journal of Chemical Crystallography
Volume	26
Issue number	4
DOIs	https://doi.org/10.1007/BF01677781
Publication status	Published - Apr 1996
Externally published	Yes

Keywords

Clathrate
Octahedral framework
Pyridine
Zinc complex

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10.1007/BF01677781

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title = "X-ray crystal structure of trans-dinitratotetrapyridinezinc(II)-pyridine solvate, a clathrate compound",

abstract = "The X-ray structure of trans-dinitratotetrapyridinezinc(II) · 2 pyridine has been determined. Clear colorless crystals of the complex crystallize in the orthorhombic space group Occa, with cell dimensions a = 12.108(3), b = 14.966(7) and c = 17.113(4){\AA}; V = 3101.0(18){\AA}3 and Z = 4. Unique reflections, 755, with Inet > 3σ (I) on refinement afforded values of R = 0.069 and Rw = 0.075.",

keywords = "Clathrate, Octahedral framework, Pyridine, Zinc complex",

author = "Pierre Losier and Zaworotko, {Michael J.}",

year = "1996",

month = apr,

doi = "10.1007/BF01677781",

language = "English",

volume = "26",

pages = "277--280",

journal = "Journal of Chemical Crystallography",

issn = "1074-1542",

number = "4",

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T1 - X-ray crystal structure of trans-dinitratotetrapyridinezinc(II)-pyridine solvate, a clathrate compound

AU - Losier, Pierre

AU - Zaworotko, Michael J.

PY - 1996/4

Y1 - 1996/4

N2 - The X-ray structure of trans-dinitratotetrapyridinezinc(II) · 2 pyridine has been determined. Clear colorless crystals of the complex crystallize in the orthorhombic space group Occa, with cell dimensions a = 12.108(3), b = 14.966(7) and c = 17.113(4)Å; V = 3101.0(18)Å3 and Z = 4. Unique reflections, 755, with Inet > 3σ (I) on refinement afforded values of R = 0.069 and Rw = 0.075.

AB - The X-ray structure of trans-dinitratotetrapyridinezinc(II) · 2 pyridine has been determined. Clear colorless crystals of the complex crystallize in the orthorhombic space group Occa, with cell dimensions a = 12.108(3), b = 14.966(7) and c = 17.113(4)Å; V = 3101.0(18)Å3 and Z = 4. Unique reflections, 755, with Inet > 3σ (I) on refinement afforded values of R = 0.069 and Rw = 0.075.

KW - Clathrate

KW - Octahedral framework

KW - Pyridine

KW - Zinc complex

UR - http://www.scopus.com/inward/record.url?scp=0030534234&partnerID=8YFLogxK

U2 - 10.1007/BF01677781

DO - 10.1007/BF01677781

M3 - Article

AN - SCOPUS:0030534234

SN - 1074-1542

VL - 26

SP - 277

EP - 280

JO - Journal of Chemical Crystallography

JF - Journal of Chemical Crystallography

IS - 4

ER -

X-ray crystal structure of trans-dinitratotetrapyridinezinc(II)-pyridine solvate, a clathrate compound

Abstract

Keywords

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